- Université Paris-Saclay, CEA, List, Palaiseau, France
Pipe internal pressure measurement is of utmost importance in the oil & gas industry to monitor the extraction process, and thus to prevent hydrate-plugs formation which may occur in specific temperature and pressure conditions. Traditional solutions usually rely on pressure sensors in direct contact with the fluid to monitor, therefore requiring one hole per sensor, but they also weaken the pipe structure, which may prematurely lead to significant leaks. Attempts to develop non-intrusive pressure sensors relying, for instance, on acoustic waves detection or even strain measurements (the pipe wall acting, in some way, like the membrane of a traditional intrusive sensor), are up to now not fully satisfying, mainly due to poor temperature cross-sensitivity compensation. Thus, 1 °C temperature compensation error typically leads for Fiber Bragg Grating (FBG) transducers to pressure measurement biases greater than 26% at 100 bar (e.g.: Ø 4” NPS Sch. 160 steel pipe). Consequently, if such non-intrusive, but biased, solutions could possibly have been considered to monitor, for instance, a Nuclear Power Plant (NPP) primary coolant circuit, it was with the risk of dramatic consequences since the fluid can reach temperatures up to 320 °C. On the other hand, the solution detailed here truly achieves to cancel the temperature cross-sensitivity, and potentially any additional effect on pressure measurement, provided that each effect has the same influence on all transducers. It first relies on a better understanding of the pipe behavior under hydrostatic pressure, supported by a dedicated model developed on purpose, which demonstrates that the internal pressure and the surface temperature variations of a closed pipe can be recovered with at least two direction-sensitive transducers, the temperature dependence of the pressure measurement being simply removed by a straightforward compensation process. This paper explains the underlying principle, thanks to a formal model established with only few hypotheses, but extended to more complex field conditions. It ends with a lab-test validation involving FBG transducers attached to a pressure circuit submitted to temperature variations greater than several tens of °C, and concludes about the advantages and limitations of this novel approach for non-intrusive sensing, and its potential extensions to other measurement techniques.
1 Introduction
Non-intrusive measurements first aim at keeping structures integrity safe while providing relevant information from their external surface. In the oil & gas industry, the monitoring of internal pressure and temperature of pipelines is necessary to prevent hydrate-plugs formation (Barker and Gomez (1989)) since it can interrupt the extraction process, with potentially significant economical and environmental consequences.
Non-intrusive measurements also make it possible to consider local inspections without any downtime, with external sensors installed and then removed on-demand from the structures to monitor, which is a key parameter for a widespread use in subsea environment.
Water distribution networks and Nuclear Power Plants (NPP) are two other examples where pipe structural integrity is equally important, with wider temperature ranges and additional ionizing radiations in the latter case, this is why non-intrusive measurement techniques must be proven reliable and safe by design.
However, none of the previous attempts to develop such non-intrusive pressure sensors has been satisfactory so far, because some of the underlying measurement principles, mainly based on ultrasonics or strain measurements, still suffer from shortcomings in their implementation.
Ultrasonic measurements already depend on many parameters, at least stresses and temperature (Salama and Ling (1980)), but the pipe dimensional changes must also be taken into account if the measurement principle relies on the analysis of the acoustic path length variations.
Diodati (1986) showed a linear dependence between the amplitude of an acoustic pulse propagating in a cylindrical vessel wall and its internal pressure, but also experienced a dependence on the compressibility of the fluid to monitor, making this measurement method unsuitable for general purpose on field.
Zhou et al. (2016) improved this technique thanks to propagation time measurements of multiple longitudinal waves propagating in the vessel wall, between several transducers located at precise positions along the pipe. But this technique also requires calibration in order to mitigate the temperature influence on pressure measurement.
From the mechanical point of view, the underlying principle usually relies on surface strains measurement, the pipe playing the role of the membrane of the traditional sensor, with strains proportional to the applied pressure in the elastic range. It has the advantage over ultrasonics not to depend on the fluid properties, but on its sole mechanical action on the pipe internal surface. But any uncontrolled mechanical effect other than hydrostatic pressure is also liable to introduce a significant pressure measurement bias.
Meiring et al. (2016) proposed to use FBG (Fiber Bragg Grating) transducers placed helically around the pipe, with a first transducer attached to it, sensitive to both strains and temperature, and a second one, loose, for temperature compensation. However, this solution only overcomes the thermal dependence of the optical fiber refractive index, on which the Bragg wavelengths depend; the pipe thermal expansion also must be compensated, as long as there is differential thermal expansion with regards to the optical fiber.
Roussel et al. (2019) adapted the original thermal compensation principle from Magne et al. (2005)1, mainly due to installation (lack of space) issues, with a loose temperature compensation FBG transducer located in a micro-tube (thus introducing the same measurement bias vs. temperature as Meiring et al. (2016)), and two additional FBGs in rosette configuration (Ferdinand et al. (1994); Magne et al. (1997)) dedicated to strains measurement once attached to the pipe surface.
But the thermal inertia discrepancy between the strains and the temperature compensation sensors also inherently introduces a bias, notably in case of rapid pressure changes (this is the same for Meiring et al. (2016)—see Table 4 for some orders of magnitude).
Last, Ekechukwu and Sharma (2021) demonstrated a well-scale distributed pressure measurement based on fiber optic DAS (Dynamic Acoustic Sensing) and DTS (Distributed Temperature Sensing), and the analysis of the DAS low-frequency components which are sensitive to both strains and temperature perturbations. Then, a machine learning process is used to predict the pressure along the optical fiber. This method produces incredibly nice results, but is not fully adapted to rapid temperature changes, and may be questionable if the fluid does not flow.
Some of these solutions (Magne et al. (2005); Zhou et al. (2016)) also suffer from the approximation of the thin-shell theory, which is not accurate enough to describe the gradients inside the pipe wall (radial stress σrr can typically range from 300 bar down to the atmospheric pressure over only a few centimeters in metallic pipes), nor the right strains values on pipe surface (recipes from materials’ strength rules are very often the results of averaged calculations over pipe sections for the relevant parameters).
The solution proposed by Adams et al. (2018), based on two FBG transducers attached in hoop & longitudinal directions, falls into this trap: even if the temperature cross-sensitivity compensation principle is correct (however similar to Maurin et al. (2007)), the thin-shell theory is also not applied correctly either, with a confusion between the concepts of “absolute pressure” and “pressure variation between two states” (the FBG transducers are used for measurements relative to a known reference state), these shortcomings being hidden by a compulsory calibration process.
This is why to overcome the drawbacks of the previous attemps to develop a non-intrusive pressure sensor, the temperature dependence of the pressure measurement must first be solved, while relying on a better description of the pressurized pipe behavior between two thermomechanical states.
2 Preliminaries Specific to Purely Mechanical Measurements
Transducers usually exhibit a cross-sensitivity with temperature; this is the case for the traditional electrical strain gauges, but also for the Fiber Bragg Gratings in the field of strain measurements.
One solution to circumvent the temperature influence on the desired mechanical measurement is simply to make the difference between the raw measurements provided by two transducers attached to the structure: as long as they exhibit the same sensitivity to temperature and are subject to its same influence, there is indeed a chance to take advantage of at least the transverse Poisson effect to get a non-zero difference value, thus only sensitive to the mechanical deformation of the structure.
One key parameter is the strains distribution in the structure at the location of each transducer, which may be complex since it depends on many parameters such as its geometry and the stresses applied onto it. But if for instance, the structure is a cylinder with circular cross-section
where E is the Young’s modulus and ν the Poisson’s ratio of the cylinder, with a positive difference in case of elongation:
FBG transducers are mainly sensitive to strains in the direction of the optical waveguide of the optical fiber, and are therefore good candidates for such selective measurements.
This principle to get rid of the temperature influence on the strains measurement, already described by Maurin et al. (2007) in case of bending, is however not fully adapted to pressure measurements for pipes, mainly because:
• the longitudinal and the hoop strains of a closed pipe behave the same with its internal pressure Pint (which results in inflating the pipe):
and make Eq. 1, by itself, inadequate for pressure measurement:
• the strains sensitivity depends on pipe thickness and diameter, which are two other parameters to be taken into account to explain the relationship with the internal pressure.
The dedicated model developed hereafter (Sections 3 and 4) takes advantage of the same temperature compensation principle (by subtraction of two raw measurements), but with transducers located at different locations on the pipe surface (unlike the solution for bending described by Maurin et al. (2007)), and also facilitates the establishment of rules to compensate for other additional mechanical effects, such as pure bending (Section 4.2), thanks to a better understanding of the pipe behavior under hydrostatic pressure.
This type of measurement is also more suitable for rapid pressure and temperature changes as long as the transducers are similarly attached to the structure, e.g.: glued: then, they behave in the same way with temperature, their inertia being mainly controlled by the thermal properties of the structure (Section 4.1.3.2.3).
Last, thermal sensitivities, for both transducers and pipe, no longer interfere significantly with the pressure measurement, which is also an improvement over previous methods involving FBG transducers (Magne et al. (2005); Meiring et al. (2016)), and therefore leads to better results (Section 5).
3 The Simplified Thermomechanical Model
The principle is to develop a thermomechanical model of a straight pipe section submitted to simple mechanical stresses and forces, leading to the expressions of the strains and stresses tensors components on its external surface, then to establish the relationship for their measurement with transducers like e.g.: FBGs between two thermomechanical states, to finally get the variation ΔPint of its internal pressure (Section 4.1.3.2).
The generalization of this model to additional mechanical sollicitations like pure bending, based on the principle that in the elastic domain, all contributions are cumulative, follows (Section 4.2.2.2).
3.1 Mathematical Description of the Thermoelastic Behavior of the Infinitely Long Pipe
The description of the pipe behavior is obtained by means of the formulation of the mechanical problem in terms of displacements. This method is different from Timoshenko and Goodier (1970) with the Airy’s function, but leads to quite the same results. The underlying hypotheses are also fully described and let the door open for a better or easier consideration of the temperature distribution in the pipe wall (Section 6).
This method first permits to calculate the components of the mechanical strains tensor, then the components of the stresses tensor (according to the Hooke’s law as long as the pipe behavior remains elastic).
The fundamental equation of dynamics for deformable bodies then leads to a set of partial differential equations, with integration coefficients expressed as functions of boundary conditions (internal and external hydrostatic pressures Pint and Pext, the longitudinal force
3.1.1 Schematic Description of the Pipe Under Hydrostatic Pressure
The mechanical sollicitations of the pipe, supposed to be infinitely long, can be modelled as described in Figure 1:
• a radial stress σrr resulting at least from the hydrostatic pressures Pint and Pext applied respectively on the inner (at rint) and the outer (at rext) pipe surfaces:
• a longitudinal stress σzz representative of the external longitudinal force
For the sake of simplicity, but also because it is a few orders of magnitude lower than the hydrostatic pressure, the shear stress σrz (which may result from friction of the fluid flow on the inner pipe surface) is neglected.
This description will also help to correctly define the boundary conditions applied to the pipe, in order to solve the set of partial differential equations resulting from the mechanical balance.
The principle is first to establish the mathematical form of the displacement vector
3.1.2 Simplifications in Axicylindrical Symmetry, Displacements and Strains Tensor
The displacement vector
The usual assumptions in terms of axicylindrical symmetry, infinite pipe length, absence of torsion, isotropic material properties and temperature homogeneity, then lead to the simplified expressions of the displacement vectors
α is the thermal expansion coefficient of the pipe, and K0 a first integration coefficient.
The linearized Green-Lagrange mechanical strains tensor
3.1.3 The Stresses Tensor and the Mechanical Equilibrium of Forces
The pipe is supposed to be used in its nominal range of deformation, typically one order of magnitude below its yield strength, so the Hooke’s law for elastic bodies applies:
The fundamental equation of dynamics for deformable bodies:
applies with the assumptions of negligible volume forces and static conditions, and then leads to the set of two partial differential equations:
3.1.4 Formal Expressions of the Displacements, Strains and Stresses in the Pipe Wall
Set of partial differential Eq. 12 is solved by separation of variables r and z for the mechanical displacement
then to the formal expressions of the mechanical strains tensor
and last to the formal expressions of the stresses tensor
3.1.5 Boundary Conditions–First Order Linearized Solution
Boundary conditions are as follows:
1. no shear stress is applied on the outer pipe surface:
2. both mechanical wσ and thermal wT longitudinal displacements are arbitrary equal to zero at z = 0 on the pipe outer surface:
3. the hydrostatic pressure Pint is applied on the pipe inner surface:
4. the hydrostatic pressure Pext is applied on the pipe outer surface:
5. the longitudinal stress σzz acting on the pipe cross-section results in the longitudinal force
6. the initial inner radius
7. the initial outer radius
3.1.5.1 First Four Integration Coefficients
The resolution of boundary conditions Eqs. 16, 17 first leads to:
and to the expression of the mechanical
for the mechanical
and for the diagonal stresses tensor
In particular, these first intermediate integration coefficients do not depend on the pressure states, nor the longitudinal force applied on the pipe, and the expressions given by equations sets Eqs. 24–26 are exact (with respect to the assumptions from the previous paragraphs, at thermomechanical equilibrium).
But the last three integration coefficients K1, L1 and L2 do depend on the pressure states and the longitudinal force, and at a lesser extent on temperature. It is necessary to take it into account later on for transducers measurements, which are always relative to an initial reference state.
3.1.5.2 Last Three Integration Coefficients–First Order Approximation
Unfortunately, the last boundary conditions do not admit any formal solution for
Boundary conditions Eqs. 18–20, combined with first order approximations Eq. 27 of rint and rext, then lead to the set of first order linearized solutions for the last three integration coefficients (E is the Young’s modulus, and ν the Poisson’s ratio):
The set of solutions Eq. 28 can be used with equations sets Eqs. 24–26 to get a first valid approximation of displacements, strains and stresses tensors components anywhere in the pipe wall.
This model is valid for all dimensions of pipes and not limited to thin-shells, and brings essentially the additional information of temperature dependency (Timoshenko and Goodier (1970)), and later on, for the closed pipe with the longitudinal force
Also, the model accuracy improvement, based on a step by step correction of the current radiuses rint and rext, is more easily taken into account, with better results with temperature (Section 3.2).
3.2 Formal Model Accuracy Improvement–Iterative Algorithm
The model accuracy for the desired parameter is evaluated by comparison of its exact solution computed numerically by solving (Marquardt (1963)) the non linear set of boundary equations (Section 3.1.5) leading to the exact values for the set of integration coefficients
Then, the improvement of this first order formal model is based on an iterative algorithm, leading to more and more accurate formal approximations for the exact values of the coefficients
This algorithm simply relies on a step by step improvement of the current inner rint and current outer rext radiuses approximation Eq. 27.
3.2.1 Iterative Improvement of the Formal Model Applied to the Internal Pressure Pint
The iterative procedure to correct the bias of the first order formal solution is described as follows:
1. initialization of radiuses
2.compute the integration coefficients
3.compute the internal pressure
4.for each step i ≥ 0:
a. correct the radiuses approximations
value for
where ϵ is an arbitrary small positive number, for instance:
5. the desired internal pressure Pint value is the last computed iterative
This algorithm can be applied similarly for the computation of any other parameter like the strains or stresses tensors components in the pipe wall, but also for the variations of such components between two thermomechanical states of the pipe (Section 4).
However in this latter case, the procedure has to be adapted to take into account the variations of each component between the two thermomechanical states.
3.2.2 Accuracy of the Formal Model for Internal Pressure Pint Measurement
The accuracy of the formal model is illustrated hereafter for the internal pressure measurement Pint between 0 bar and 150 bar and between 0°C and 320°C, according to boundary condition Eq. 18.
The relative errors of the iterative model are presented for Ø 2″ NPS Sch. 80 and Ø 4” NPS Sch. 160 steel pipes, and are computed as follows:
The results, illustrated in Figure 2 for these two steel pipes with transducers in hoop & longitudinal configurations, show that the maximum relative error is observed for the first order linearized solution (computed with integration coefficients Eq. 28), at the maximum pressure (150 bar) and temperature (320°C):
• for the Ø 2″ NPS Sch. 80 steel pipe, the model accuracy is better than 0.147%,
• for the Ø 4” NPS Sch. 160 steel pipe, the model accuracy is better than 0.109%.
FIGURE 2. Iterative model relative error for Pint, from initialization (linear approximation–order 1) to iteration 2 (order 3) (Pref = 0 bar and Tref = 0°C)—First row: Ø 2″ NPS Sch. 80 steel pipe–Second row: Ø 4” NPS Sch. 160 steel pipe.
The accuracy of this algorithm, which corrects at each iteration the current pipe inner and outer radiuses approximations (Eq. 27), and therefore the radial forces resulting from the inner and outer hydrostatic pressures, is typically improved by three orders of magnitude from one iteration to another (Figure 2).
However, the first order linearized solution, with integration coefficients (Eq. 28), is accurate enough for most applications (i.e.: metallic pipes), but this iterative algorithm will be particularly useful for highly deformable structures (e.g.: Composite Overwrapped Pressure Vessels (Maurin et al. (2014))).
The other main advantages of the iterative algorithm is its simplicity (well suited to lightweight implementations) and its very fast convergence (a few iterations are enough).
4 Application to Non-intrusive Pressure Variation Measurements
The first step is to establish the relationships between two different thermomechanical states of the pipe, and their respective boundary conditions.
The second step is to connect these relationships to the raw measurements performed by the transducers.
4.1 Recipe for Pressure Variation Measurement
The recipe for pressure variation measurement is to make use of the set of linearized solutions (Section 3.1.5.2) between two thermomechanical states, considering that:
1. the reference measurement is performed at known temperature T0, hydrostatic pressures Pint and Pext, and longitudinal force
• this measurement is associated to the first set of coefficients
2. the current measurement is performed at unknown temperature T0 + ΔT, hydrostatic pressures Pint + ΔPint and Pext + ΔPext, and longitudinal force
• this measurement is associated to the second set of coefficients
These two sets of coefficients,
For FBG transducers, this physical parameter is the mechanical strain, therefore these constants must be used with the expression of the strains tensor described by equations set Eq. 25.
4.1.1 Pressure Variation Measurement Expressed in Terms of Strains
The resolution of the two sets of boundary conditions is a three steps process:
1. the relationship between the absolute strains measurement ɛ (formulae established so far) and the relative strains measurement Δɛ (performed by the transducers between two different thermomechanical states) is first described:
2. then, the difference (Eq. 33) is expressed according to the relative hoop Δɛθθ and longitudinal Δɛzz strains measurements given by the transducers attached to the pipe external surface (at radius rext):
3. last, the set of Eq. 34 is solved in terms of ΔPint and ΔF:
It has to be underlined that solution Eq. 35 is valid whether the pipe is closed or not.
4.1.2 Link With the Raw Measurements–The Fiber Bragg Grating Transducer
The raw measurement performed by a transducer usually exhibits a cross-sensitivity with temperature; this is the case for the FBG which acts as a narrowband mirror filter in wavelength, with characteristic reflected first order wavelength λB (Martinez (1999)):
which differentiates as follows:
where:
•dT is the infinitesimal temperature variation at the exact FBG location,
•dɛmec is the infinitesimal longitudinal mechanical strain variation at the exact FBG location,
•
•
•
•
It leads to Eq. 37, with coefficients values valid for a germanosilicate optical fiber5:
Provided that the optical fiber is correctly attached to the structure6, the total (mechanical + thermal) strains variations, for both the optical fiber and the structure, are equal:
then, it is correct to rewrite Eq. 38 from the point of view of the mechanical strains of the structure:
with an apparent FBG temperature sensitivity
According to these expressions (depending on whether it has to deal with the mechanical strain of the optical fiber or the structure), the Bragg relationship dedicated to temperature and strain measurements can be written, after integration and with the hypothesis of κɛ and κT constant sensitivities:
which is rewritten as follows:
with a true relative variation measurement
and a mechanical strain Δɛmec such as:
The notation
From now on, the mechanical strain variation Δɛmec measured by the transducer is assumed to be the mechanical strain variation of the structure to which it is attached to, as described by Eq. 40, with sensitivities κT and κɛ such as:
If all transducers are similarly attached to the structure (from the thermal and mechanical points of view), it can be assumed that there is almost no dispersion between each sensitivity coefficient
and it is possible to make the same assumption for all the products
Thus, if two FBG transducers are respectively oriented with angles φ1 (defining
FIGURE 3. Definition of the FBG transducers angles φ1 and φ2 associated to vectors
which leads to
and to their expression in terms of true relative raw transducer
and therefore to:
4.1.3 Temperature Self-Compensated Pressure Variation Measurements
The temperature variation ΔT is seamlessly introduced in the previous sets of equations with the temperature transducer cross-sensitivity κT, thus making the use of an additional sensor unnecessary.
According to the set of Eq. 35, the only way to solve the temperature dependency is through the expression of the longitudinal force. Two cases can be distinguished:
1. if the longitudinal force variation
2. if the pipe is closed (Section 4.1.3.2).
In both cases, the hypotheses of identical temperature sensitivities8 and temperature ΔT variation must be verified.
4.1.3.1 Solution in Case of Known Longitudinal Force Variation
The second equation of set (Eq. 52) combined with the second equation of set (Eq. 35) lead to the expression of temperature ΔT variation in terms of longitudinal force ΔF and external pressure ΔPext variations:
which used in combination with the first equation of set (Eq. 52) and the first equation of set Eq. 35, leads to the internal pressure variation ΔPint:
Thus, assuming known longitudinal force ΔF and external pressure ΔPext variations, internal pressure ΔPint (Eq. 54) and surface temperature ΔT (Eq. 53) variations can be obtained by means of non-intrusive measurements, without any additional extrinsic sensor to compensate for transducers temperature cross-sensitivity.
Eqs. 53 and 54 are valid whether the pipe is closed or not. However, the value of the longitudinal force variation ΔF is very often not known. Moreover, if the pipe is closed, its internal pressure also acts as a longitudinal force (Section 4.1.3.2).
4.1.3.2 Solution for the Closed Pipe
If the pipe is closed, which is the majority of field cases9, the longitudinal force variation ΔF is expressed as follows10:
approximated by:
and used in combination with Eqs. 53, 54, gives the first order linearized expression of the internal pressure ΔPint and surface temperature ΔT variations for the closed pipe:
4.1.3.2.1 Properties of This Non-intrusive Pressure ΔPint Variation Measurement
Equations set (Eq. 57) first demonstrates, as already suggested in Section 2, that only one pair of transducers is necessary for the non-intrusive pressure ΔPint and surface temperature ΔT variations measurement11, with orientation angles φ1 and φ2 such as:
with the maximum sensitivity for pressure measurement obtained for:
The temperature compensation process for purely mechanical measurement is straightforward, by simple subtraction of two true relative variation of raw transducers measurements.
This also implies that any additional physical phenomenon which has the same effect on the raw measurement performed by each transducer can be expected to be optimally mitigated (e.g.: nuclear radiations on Bragg wavelengths) by the same compensation process.
In this case, the effects of additional physical phenomena are combined to those of temperature. Then, the second equation of set Eq. 56 has to be interpreted in terms of “combined additional effects other than purely mechanical”, with a specific global sensitivity (a priori different from κT used until now for temperature only) depending on the instantaneous relative ratios and intensities of any of these additional phenomena.
4.1.3.2.2 Comments on a Possible Thermal Dependency of the Non-intrusive Pressure ΔPint Variation Measurement
First equation of set Eq. 57 also demonstrates that this pressure measurement does not depend on the pipe, nor the transducer thermal properties anymore: it is therefore independent from any external temperature variation influence (provided that all the underlying hypotheses are fulfilled, especially in terms of identical thermal sensitivities
This is all the more true since the surface temperature (where the transducers are located), in applications with metallic pipes, is mainly weighted by the thermal effusivity a of the structure, defined as follows:
As a reminder, at thermal equilibrium, two semi-infinite media in flat contact have the temperature
In other words, and according to Table 1, if the transducers are attached to the external surface of a stainless steel 310 pipe surrounded by air or water, its contact temperature
TABLE 1. Thermal effusivities at 25 °C and 1 bar calculated from physical properties (for air, water and stainless steel 310—from Rumble (2021)).
4.1.3.2.3 Comments on the Associated Surface Temperature ΔT Variation Measurement
The associated pipe surface temperature ΔT variation measurement described by Eq. 57 corresponds in fact to the contact temperature
In order to get a more accurate pipe wall temperature ΔTwall variation (especially if the surrounding medium is water), Eq. 61 has to be solved, which leads to:
but this requires the additional temperature ΔText variation measurement of the surrounding medium.
Thermal effusivities ratios given in Table 2 confirm that the temperature correction introduced by Eq. 62 will actually remain small in most cases.
4.2 Pressure Variation Measurements Free From Pipe Bending
The model established so far relies on the hypothesis of an infinitely long and straight pipe (Section 3.1). However on field, the pipe is submitted to many different external forces which may lead to bending, thus potentially introducing significant measurement biases.
But it is still possible to cope such biases while using the same formal model dedicated to straight pipes if some hypotheses are fulfilled.
4.2.1 Mechanical Strains due to Bending
The mechanical strains in the bended pipe can be described by Figure 4. The associated coordinate system is the Cartesian coordinate system
FIGURE 4. Bended pipe–Relationship between the local Cartesian coordinate system
Without any other longitudinal force than those applied by the internal and external hydrostatic pressures (Eq. 55 for the closed pipe), the neutral flexural surface is located exactly at half height of the pipe. When the longitudinal force variation is not null
with a longitudinal stress component variation
which leads to the equilibrium equation expressed in terms of ΔF and the two curvature radiuses R and Rref:
In the local cylindrical coordinate system
in the cylindrical coordinate system(O, r, θ, z)
The set of mechanical strain components (Eq. 66) can be added to the components of the previous model developped in Section 3.1 for the infinitely long and straight pipe, to give, at radius r in the pipe wall, the resulting mechanical strain
Equation 67 introduces at least three additional parameters (R, x0 and θR), which complicates the formal resolution of the problem in terms of pressure, and the first temptation is to solve it numerically (with the appropriate number of independent strain measurements corresponding to at least the same number of independent equations of type Eq. 67).
4.2.2 Specific Solutions if the Neutral Flexural Surface Passes Through the Pipe Axis
The idea is to get rid of the influence of bending by noticing that it generates both compressive and tensile stresses over all its cross-section. The summation of each of these contributions, when the transducers are properly positioned, should therefore lead to the cancellation of their global contribution.
And one way to distribute the transducers around the pipe is evenly.
4.2.2.1 Benefits of Uniformly Distributed Measurements Around the Pipe
If the neutral flexural surface passes through the pipe axis (i.e.:
This method has the major advantage to be free from the relative angular position θR of the osculating plane for each point M (Figure 4) which no longer needs to be known. In the general case, Eq. 66 leads by averaging to:
Thus, as long as the neutral flexural surface passes through the pipe axis, the average of the mechanical strains in bending is equal to zero if the pairs of transducers are evenly located around the pipe (Figure 5), which implies, taking into account equations set Eq. 66:
FIGURE 5. N pairs of transducers evenly arranged around the pipe, every θN = 2π/N (N ≥ 2), to get rid of the bending effects by summation of their mechanical strains variation measurement – Examples for N = 3 (left) and N = 6 (right).
Then, Eq. 67 can be used for the mechanical strains variation measurement corresponding to the N pairs of FBG transducers evenly located, every θN = 2π/N around the pipe:
According to this last expression, the mechanical strain variation corresponding to pure bending is equal to zero as long as each transducer is oriented with the same angle φ0 or − φ0; thus:
The additional condition on φ0 leading to
1. this non-intrusive measurement requires at least one pair of transducers, thus if the first transducer angle φ1 already satisfies the equation
2. Poisson’s ratio ν must be known with precision, which is rarely the case for a pipe already on field.
However, this additional condition on angle φ would have been probably a good idea to mitigate the bending effect on the pressure measurement if the transducer was already natively temperature insensitive (thus, only one transducer providing a purely mechanical measurement would have been necessary).
But this is another topic, out of the scope of this paper.
4.2.2.2 Recipe for Pressure Variation Measurement in Case of Additional Bending
As long as the N pairs of transducers are evenly distributed around the pipe (every θN = 2π/N), and according to Eq. 71, the mechanical strains variations due to pure bending are eliminated if the average mechanical strain variation
with:
Solutions of equations sets Eqs. 72, 73 are essentially the same than without bending, with a single pair of transducers measurement, the average measurements replacing the single measurement as long as the N pairs of transducers are all oriented with the same couples of angles
Thus, equations set Eq. 57 is adapted for N ≥ 2 pairs of transducers evenly arranged around the pipe:
However, this set (Eq. 74) of solutions is valid only if the neutral flexural surface passes through the pipe axis, which implies the additional hypothesis of pure bending, hence δF = 0.
If δF ≠ 0, several additional parameters must be known with precision as long as the transducers are temperature sensitive: the curvature radiuses, the orientations of the osculating planes and the positions of the neutral flexural surfaces in both the reference and the current thermomechanical states (Section 4.2.1).
5 Experimental Validations
The measurement method disclosed in this paper has been validated experimentally. Three lab-tests are presented hereafter:
1. the first test involves a closed pipe with no external force applied on it: it enables to have a first look to its bare performances in terms of pressure measurement accuracy, once calibrated (Section 5.1),
2. the second test involves an air pressure loop controlled by flow rate, very similar to an industrial installation: it demonstrates the ability of this measurement principle to get a realistic pressure variation measurement (interpretable in terms of pressure drop) directly correlated to an air flow rate (Section 5.2),
3. the last tests involve a water pressure loop dedicated to reproduce a Nuclear Power Plant (NPP) primary coolant circuit, with wide temperature and pressure changes, in order to push to its limits this non-intrusive measurement principle (Section 5.3).
For all these tests, one FBG is oriented with φ = π/2, thus sensitive to the longitudinal mechanical strain
All transducers were attached to the pipe surface with a thin film of glue, and except for the last test (Section 5.3.3), FBGs were in direct contact with the surrounding air, at room temperature.
Bragg wavelengths were recorded with a commercial measurement system from Micron-Optics™, model Si255 (and all FBGs are quite standard FBGs, from mass-market production).
5.1 Bare Performances of the Non-intrusive Pressure Variation Measurement Evaluated on a Mechanically Isolated Pipe
This test involves an experimental setup including a closed pipe with the following characteristics:
This pipe is equipped with a reference pressure sensor in direct contact with the fluid (some water), and a dedicated external hydraulic circuit is in charge of its pressurization (Figure 6). This pressure testing facility is located at Technip Energies in Marseille (France) and enables to inflate the pipe up to 300 bar.
FIGURE 6. Detailed view of the water pressure testing facility at Technip Energies in Marseille, with two FBG transducers glued on the pipe external surface.
The FBG raw measurements, leading to internal pressure variation
The two pressure data sets are post-synchronized once the error function
The pressure test held in Marseille in July 2019 consisted in several pressure steps up to 300 bar (Figure 7). The sampling rate of the reference pressure measurements
The average quadratic FBG measurement error
Between the minimum pressure
It has to be noticed that the FBG surface temperature variation ΔTFBG (computed with the standard Poisson’s ratio (Eq. 75)) varies in opposite to the reference thermocouple temperature ΔTTC (Figure 8, left). This may be due to at least two reasons; formula for temperature variation ΔT in equations set (Eq. 57):
• depends on the Poisson’s ratio ν, which is often not known with the adequate accuracy for all structures,
• is valid at thermomechanical equilibrium with the underlying hypothesis of an homogeneous temperature in the pipe wall.
FIGURE 8. Results of the pressure test held at Technip Energies facility in Marseille in July 2019—With additional surface temperature variation computed from FBG measurements (ν = 0.3 (left) and ν = 0.35 (right)).
After manual adjustment of the Poisson’s ratio, set to ν = 0.35 (which is an over-estimated value for steel) in the second equation of set (Eq. 57), this discrepancy was reduced by a factor of four (Figure 8 right), with no impact on pressure measurement average error
and for this specific pressure test:
which is a valid value for steel.
Anyway, such temperature measurement should be considered with limited confidence out of thermal balance, at best as indicative only, especially since it depends on the mechanical properties of the structure (but other kinds of FBG transducers–on their side, totally decorrelated from the strains of the structure to which they are attached to–may provide this measurement in a better way (Roussel et al. (2018))).
5.2 Non-intrusive Pressure Variation Measurement on an Air Pressure Loop
The second type of validation occured in October 2019 on an air pressure loop controlled by flow rate (Mercure facility located at CEA in Cadarache, France). The main advantage of such test facility, for the qualification of the non-intrusive measurement, is its complexity in terms of pipe layout, including several bends (Figure 9), then potentially leading to additional external forces acting on the pipe, such as:
• longitudinal forces due to differential thermal expansion between the pipe and its attachments,
• bending forces due to the changes in air flow rate or/and direction when crossing each bend.
FIGURE 9. Mercure air pressure loop facility (DES, CEA/Cadarache)—Overview of the pipe layout (left) and detailed view of FBG transducers installation on pipe surface (right).
The FBG transducers are located in the middle of a 5 m long pipe section. The pipe characteristics are described hereafter:
The optical measurements were performed at 5 kHz, then averaged to 2.5 Hz to improve the signal to noise ratio (Figure 10 left). The flow rate Q is measured with a Rosemount™ flowmeter device:
FIGURE 10. Air flow rate steps and corresponding FBG non-intrusive pressure variation measurement vs. time (left) and non-intrusive pressure variation vs. air flow rate measurements (right) on Mercure facility.
Measurements are reported in Table 3 (Reynolds number is greater than 9,600—the flow is turbulent).
FBG pressure variation ΔPFBG vs. air flow rate Q (Figure 10 right) is very similar to pressure drops which can be calculated from recipes for natural gas pipelines (e.g.: Coelho and Pinho (2007)), with a clearly univocal relationship of pressure drop vs. air flow rate, which confirms the relevance of this non-intrusive measurement method in such situation.
5.3 Non-intrusive Pressure Variation Measurement on a Water Pressure Loop
The last experimental tests were performed at BEARN 2 facility in Saclay (France). This water pressure loop enables flow rates up to 14 m3/h with temperatures up to 320 °C, and pressures up to 150 bar. The pipe layout includes several bends and attachments (Figure 11).
FIGURE 11. CEA BEARN 2 pressure loop facility (left) and detailed view of a typical attachment (right).
All non-intrusive FBG pressure measurements were performed with standard thermomechanical values for steel (E = 195 GPa, ν = 0.3 and α = 16.4 × 10–6 K−1).
In order to put the next results into perspective, some orders of magnitude have been estimated from Eqs. 41, 57: if δλB = 1 pm is the Bragg wavelength resolution, and δPint = 1 bar the pressure measurement resolution target, they highlight that the most critical parameter is the FBG temperature cross-sensitivity compensation process (Table 4), which has to be as efficient as possible.
TABLE 4. Orders of magnitude for standard FBG transducers attached on pipe surface, operating at λB = 1550 nm (with E = 195 GPa, ν = 0.3 and α = 16.4 × 10−6 K−1 for steel).
5.3.1 Pressure Variation Measurements at Constant Temperature, No Flow
The first test was performed on a Ø 4” NPS Sch. 160 pipe section.
Without any flow, the water temperature remained constant, so the thermal differential expansion between the pipe and its attachments (responsible for δF in equations set Eq. 57) remained under control as long as the room temperature did not change too much.
The single sensor12 pressure measurement (Figure 12 left) was calibrated during the first two and a half hours with a typical average model error equal to 1.36 bar
FIGURE 12. First pressure test with no fluid flow and fluid constant temperature (Ø 4” NPS Sch. 160)—Single sensor (left) vs. three sensors average measurements to mitigate potential bending effects (right).
The average of three sensors measurements to mitigate the potential bending effects on pressure measurement (Figure 12 right) does not improve the measurement with an absolute pressure measurement error drift close to 2 bar after 18 h of test. Additional effects other than pure bending might be suspected.
The maximum errors correspond to the rapid pressure changes between two steps, mainly due to the sampling rates difference between optical (10 Hz) and reference (every 17 s) pressure measurements.
5.3.2 Pressure Variation Measurements With Temperature Changes, No Flow
The second test involves the same section, but isolated from the other part of the pressure circuit with fluid flow. Temperature variations are due to heat conduction between the two isolated pipe sections.
The pressure measurement was calibrated at constant temperature during the first 2 hours, with a typical average model error equal to 2.12 bar
FIGURE 13. Second pressure test with no fluid flow and temperature changes (Ø 4” NPS Sch. 160)—Single sensor (left) vs. three sensors average measurements to mitigate potential bending effects (right).
Both temperature measurements behave the same way, with a limited discrepancy (a few °C) which also may be due to the temperature gradient along the pipe section since these two measurements were not performed at the same location.
The average of three pairs of sensors measurement to mitigate the potential bending effects on pressure measurement (Section 4.2.2.2) does not lead to significant better results (Figure 13 right): this might be due to additional longitudinal forces, e.g.: due to differential thermal expansion and pipe attachments.
5.3.3 Pressure Variation Measurements With Flow Rate and Temperature Changes
Transducers are now attached to a Ø 2” NPS Sch. 80 pipe section, with pressure measurements three times more sensitive to any unexplained longitudinal force variation δF (Table 4).
The other main difference is the fluid which flows up to 14 m3/h with significant friction effect, and the thermal isolation of the instrumented section.
Also, the mechanical effect of a rapid and massive fluid flow change (from 14 m3/h to zero–Figure 14) has been experienced in a more significant way than previously on the air pressure loop (Section 5.2), mainly due to the mass volume difference between air and water, therefore resulting in more important external bending forces acting directly on the pipe.
FIGURE 14. Last pressure test with fluid flow and temperature changes (Ø 2″ NPS Sch. 80)—Single sensor (left) vs. two sensors average measurements to mitigate potential bending effects resulting from massive flow change (right).
This last pressure measurement was calibrated during the first 42 min while both temperature and flow changed, with a typical average model error equal to 2 bar
The pressure measurement average error until the end of the test is equal to −8.6 bar with one pair of transducers (Figure 14 left), with fluid temperature increase up to 38 °C; the average of two measurements to mitigate potential bending effects led this time to at best twice better results (Figure 14 right).
Both temperature measurements behave the same way, with a limited discrepancy as long as the fluid flows, during the first two and a half hours.
As soon as the flow is stopped, the temperature discrepancy increases, which may be explained by the difference in heat exchange along the pipe section, these measurements being not performed at the same place. Pressure discrepancy also increases, which may be the result of a change in the mechanical efforts exerted on the pipe, since the flow change also modifies the external efforts balance.
The pumps vibrations may also have modified the mechanical balance, since the pipe is in reality partially locked in its attachments (Figure 11 right).
6 Conclusion, Discussion and Perspectives
The non-intrusive pressure variation measurement disclosed in this paper is an improvement over previous methods in terms of temperature compensation, considering that 1 bar pressure resolution typically requires a temperature compensation error better than 0.054 °C for a Ø 2” NPS Sch. 80 steel pipe (Table 4).
It is based on a formal model, which demonstrates that the pressure change in a pipe can be measured by simple subtraction of two direction-sensitive surface measurements, the temperature influence being intrinsically cancelled.
This is the result of the application of a spherical stress (the hydrostatic pressure) on a closed cylindrical structure (the pipe). This asymmetry intrinsically generates significant different mechanical strains variations in two directions (hoop vs. longitudinal), allowing the exploitation of this remarkable property for the purpose of purely mechanical measurements with only two direction-sensitive transducers, and therefore hydrostatic pressure variation measurements as long as the pipe keeps its axicylindrical geometry with a circular cross-section, and remains in its elastic domain13.
Its experimental validation in harsh conditions led to at maximum 8.6 bar pressure error, with temperature changes up to 38 °C, but also flow change from 14 m3/h to zero, thus significantly modifying the mechanical balance of the pipe layout including several bends (Section 5.3.3).
This sensor used on a straight (without any bend) pipe with constant inner section (e.g.: vertical onshore drilling), should therefore lead to more accurate non-intrusive hydrostatic pressure measurements, since in such conditions, the pipe is no longer subject to external forces that can be generated by any change in fluid flow or/and direction.
By extension, this method should also enable the mitigation of any other physical effect as long as it has the same influence on all raw measurements (Section 4.1.3.2.1): this is a key advantage for measurements in a Nuclear Power Plant, in order to mitigate the effects of ionizing radiations on transducers (even some additional work is required to validate the reliability of this non-intrusive pressure measurement in such harsh environment).
Its bare performances, better than 0.54% Full Scale
Such measurement principle could also probably benefit to other kinds of cylindrical structures, like type IV Composite Overwrapped Pressure Vessels (COPV) dedicated to high pressure dihydrogen H2 storage, since the non-intrusive hydrostatic pressure measurement, when combined with the fluid reference pressure measurement, is a crucial information to establish a Damage Assessment Parameter, with the advantages over the previous method (Maurin et al. (2014)) based on the OFDR Rayleigh backscattering technique (Froggatt and Moore (1998)), to be intrinsically temperature-compensated and compatible with real-time requirements (for instance to evaluate the vessel damage assessment status during the H2 filling process).
Anyway, the measurement bias introduced by some unexplained residual longitudinal force δF (e.g.: due to differential thermal expansions) is one limitation for an application on pipe structures, which therefore must be taken into account before any deployment. Also the additional measurement provided by other means of such longitudinal efforts, combined with the recipe to mitigate the bending effects (Section 4.2), should help to improve the accuracy for pressure measurements on field.
On their side, surface temperature measurements should be considered with limited confidence, since they also depend on the mechanical characteristics of the structure, even if the discrepancy with the reference measurements remained under control during the BEARN 2 pressure tests (Section 5.3). But this surface temperature measurement could still be used as an additional information, for instance to prevent hydrate-plugs formation during subsea oil & gas extraction (Barker and Gomez (1989)).
The formal model developped in Sections 3 and 4 can also probably be improved, first by introducing a radial temperature gradient in the pipe wall (but this would require to have a temperature measurement on the pipe inner surface … ).
The temperature κT and strain κɛ sensitivities dependency on strains and temperature, supposed to be constant in this paper, can also be introduced in Eq. 40, which should lead, after integration, to a more precise relationship than Eq. 42, thus to more accurate measurements in case of wider temperature changes.
On another level, as soon as the transducers measurement principle is orientation-sensitive, the recipes disclosed in this paper should apply.
Thus, measurement techniques like ultrasonics should be able to benefit from this work, provided that the acoustic wave propagation time Δt variation, between two thermomechanical states and two transducers, is interpreted in terms of total (mechanical + thermal) true strain variation Δɛ (Eq. 25):
The stresses tensor components described by equations set Eq. 26 should also help for better ultrasonics velocity v prediction in the pipe wall (Salama and Ling (1980)).
Last, since non-contact image correlation techniques can be applied to measure surface strains (Sutton et al. (2009)), their application to pipe structures should also enable non-contact hydrostatic pressure variation measurements relying on the recipes disclosed in this paper.
This could be a major advantage in order to perform such measurements in restricted areas where it is no more possible to enter (for example in case of a nuclear accident, after a release of fission products), and therefore install or repair sensors.
Data Availability Statement
The raw data supporting the conclusion of this article will be made available by the authors, without undue reservation in the CEA HAL open archive, as an attached compressed file to this paper, and available online at: https://hal-cea.archives-ouvertes.fr/cea-03541365.
Author Contributions
LM is the main contributor to this article, from the development of the formal model for non-intrusive pressure and surface temperature measurements with only two direction-sensitive transducers, with the elaboration of the recipe to mitigate the bending effects on pressure measurement, to the participation to all the pressure tests reported in this paper, the measurements data post-processing, their analysis, the conclusion and the discussion.
Funding
This research topic was first co-funded by the FSH14 public fund (CEP&M15 project n° 9512/01), then by TotalEnergies (contracts ref. TEPRD: FR00008107, and ref. CEA: C23466-1).
Conflict of Interest
This research topic was first co-funded by the FSH public fund (CEP&M project n° 9512/01), then by TotalEnergies (contracts ref. TEPRD: FR00008107, and ref. CEA: C23466-1, on the basis of non-standard FBG transducers) for the sole co-funding of the last pressure test on BEARN 2 facility. TotalEnergies was not involved in the study design, collection, analysis, interpretation of data, the writing of this article, nor the decision to submit it for publication. All authors declare no other competing interest.
Publisher’s Note
All claims expressed in this article are solely those of the authors and do not necessarily represent those of their affiliated organizations, or those of the publisher, the editors and the reviewers. Any product that may be evaluated in this article, or claim that may be made by its manufacturer, is not guaranteed or endorsed by the publisher.
Acknowledgments
The authors acknowledge TotalEnergies and M. Marc Baqué for their support, which permitted the rehabilitation of the BEARN 2 pressure loop, and thus to carry out the pressure tests in harsh, close to field conditions. Authors also acknowledge Technip Energies and M. Daniel Mabily for their kind permission to publish the results of the pressure test held in Marseille (Section 5.1), M. Kévin Cruz from CEA DES IRESNE for the pressure test held on Mercure facility in Cadarache (Section 5.2), M. Franck Ruffet from CEA DES DM2S for its availability during the pressure tests held on BEARN 2 facility in Saclay (Section 5.3), and the FSH public fund, which permitted to initiate the research work on the formal pressure and temperature model.
Supplementary Material
The Supplementary Material for this article can be found online at: https://www.frontiersin.org/articles/10.3389/fsens.2022.835140/full#supplementary-material
Footnotes
1Based on an additional FBG attached to a separate and unstressed piece of the same pipe material, supposed to be maintained at pipe temperature, for FBG thermo-optic and pipe thermal expansion compensations in such configuration.
2Strictly speaking, this is the product α ΔT which has to be taken into account. Also, the thermal expansion coefficient α must be known, but a rough approximation is acceptable since it has a minor impact on pressure measurement.
3See Sections 4.1.3.1 and 4.1.3.2 in case of temperature self-compensated pressure variation measurements.
4The type of mechanical sollicitation plays a role:
5Published thermo-optic coefficient
6To the extent that the mechanical strength of the optical fiber is negligible compared to the mechanical strength of the structure.
7There is no surface shear strain: Δɛrθ = Δɛθz = 0.
8It is supposed to be true if all the transducers are, for instance, glued the same way to the structure, see Eqs. 47, 48.
9For instance, in subsea oil & gas extraction, the pipe is connected on one side to the well (which is a closed volume), and on the other side to the storage station (which is also a closed volume).
10The theoretical justification can be found, for instance, in Forest et al. (2009–2010), Section 12.1.5, pp. 277–279.
11Whereas previous solution from Magne et al. (2005) and Roussel et al. (2019) requires at least one additional transducer for FBG temperature compensation.
12One sensor is defined as one pair of transducers attached to the pipe surface, compliant with Eq. 58.
13So the Hooke’s law Eq. 10 still applies, otherwise, the triaxiality of the stresses in the plastic domain, at least for metallic structures according to the von Mises’ criterion, with the additional property of iso-volume deformations (Forest et al. (2009–2010)), will then impose to develop a different thermomechanical model.
14FSH: Fonds de Soutien aux Hydrocarbures (French public fund for oil & gas research works).
15CEP&M: Comité d’Études Pétrolières et Marines (committee for oil & gas and marine studies).
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Nomenclature
Abbreviations
BEARN Boucle en Eau à l’Ambiance des Réacteurs Nucléaires (water pressure loop in nuclear reactors ambience)
FBG Fiber Bragg Grating
NPP Nuclear Power Plant
NPS Nominal Pipe Size
Sch. Schedule
Thermomechanical parameters
λ, μ Lamé’s coefficients
E Young’s modulus
ν Poisson’s ratio
α thermal expansion coefficient
a thermal effusivity
k thermal conductivity
ρ volume mass
Cp mass heat capacity
Geometrical parameters
rint current inner radius
rext current outer radius
Rref initial curvature radius
R current curvature radius
Displacement, strain and stress
ɛmec mechanical strain
ɛth thermal strain
σ stress
Boundary conditions and integration coefficients
Pint current inner hydrostatic pressure
Pext current outer hydrostatic pressure
T0 initial temperature
T current temperature
Measurements
Ψ transducer raw measurement (e.g.: λB for the FBG transducer)
ΔΨ variation of parameter Ψ between reference Ψ0 and current Ψ1 values ΔΨ = Ψ1 − Ψ0
FBG transducer
κT transducer sensitivity to temperature
κɛ transducer sensitivity to longitudinal mechanical strain
neff optical fiber waveguide effective refractive index
Λ grating pitch
λB Bragg wavelength
Keywords: non-intrusive measurement, hydrostatic pressure, pipe, oil & gas, intrinsic temperature compensation, formal model, direction-sensitive transducer, Fiber Bragg Grating
Citation: Maurin L, Roussel N and Laffont G (2022) Optimally Temperature Compensated FBG-Based Sensor Dedicated to Non-Intrusive Pipe Internal Pressure Monitoring. Front. Sens. 3:835140. doi: 10.3389/fsens.2022.835140
Received: 14 December 2021; Accepted: 14 January 2022;
Published: 27 May 2022.
Edited by:
Patrice Megret, University of Mons, BelgiumReviewed by:
Riqing Lv, Northeastern University, ChinaAsrul Izam Azmi, University Technology Malaysia, Malaysia
Copyright © 2022 Maurin, Roussel and Laffont. This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.
*Correspondence: Laurent Maurin, bGF1cmVudC5tYXVyaW5AY2VhLmZy