Zakaria Che Muda¹*

¹Department of Civil Engineering, Faculty of Engineering and Quantity Surveying, INTI International University, Nilai, Malaysia
²Department of Civil Engineering, College of Engineering, Qassim University, Unaizah, Saudi Arabia

The effects of polypropylene fibres on mortar and cement-paste cracking were investigated using different amounts of fibre fractions and eccentric rings under restrained-shrinkage conditions. Eccentric-ring tests were conducted to investigate early-age shrinkage cracks. The characteristics of restricted cementitious materials were described by evaluating the cracking time and using concrete mixtures that are less likely to crack. Different fibre-volume fractions significantly enhanced the width, area, and age of cracking. Increasing the water-cement ratio and sand percentage increased the cracking age. The eccentric-ring test showed a greater susceptibility to cracking in cement-mortar composites. The mechanical strength was assessed, and the impact of polypropylene fibres was investigated.

1 Introduction

In the concrete industry, cracking of cementitious products presents a serious challenge. The formation of cracks significantly affects not only the mechanical qualities of concrete but also its durability. Rapid penetration of harsh chemicals, enhanced carbonation, and faster corrosion of reinforcement in concrete are indicators of decreased durability. Under certain circumstances, shrinkages of cement-based materials cause internal stress during the initial stages of hydration, and may lead to cracking if the strain is not dispersed (Wongtanakitcharoen and Naaman, 2007; Choktaweekarn and Tangtermsirikul, 2009; Kanavaris et al., 2019; Idrees et al., 2022).

The American Society for Testing and Materials (ASTM) and American Association of State Highway and Transportation Officials (AASHTO) recommended confined ring tests to assess the probability of early-age cracking in mortar and other cementitious materials. However, the concentric ring test has drawbacks in that fractures and cracks appear at random locations. Additionally, the cracking duration of a specimen is significantly prolonged (Dong et al., 2014; Zhou et al., 2014; Dong et al., 2017; Kanavaris et al., 2019). New ring test techniques, such as the elliptical ring test (Dong et al., 2014; Dong et al., 2017; Dong et al., 2018) and square-eccentric-ring test (Branston et al., 2016), have been suggested as a substitute for the circular ring-test method for decreasing the ring-test time and observing the crack growth.

Reinforcing concrete with fibres significantly improves the mechanical properties, enhancing the ductility, while providing more dynamic stress resistance. Furthermore, it is a highly effective method for controlling and reducing the development of drying-shrinkage cracking (Abusogi and Bakri, 2022; Zhang et al., 2022). This method also controls and reduces the likelihood of cracks appearing because of drying shrinkage. Using fibres as a secondary reinforcing mechanism releases the tension formed during drying. It has the potential to prevent crack propagation and scabbing failures (Wongtanakitcharoen and Naaman, 2007; Banthia and Gupta, 2006; Juarez et al., 2015). It is of utmost importance to be aware of the circumstances in which a particular kind of fibre performs at its peak, as well as the volume fraction (V_f) that might minimise the overall drying shrinkage (Alavi Nia et al., 2012; Sadiqul Islam and Gupta, 2016; Saradar et al., 2018).

Polypropylene (PP) fibres are the most efficient and cost-effective type of fibres available today for concrete (Tang et al., 2018). They are also believed to be inert in high-pH cementitious environments. They are simple to disperse in cement mortar and concrete mixes. However, the precise impact of the PP fibre shape, diameter, length, fibrillations, and other factors is not completely known. Different approaches may be used to investigate the shrinkage-induced cracking in cement-based materials. The two specimens used most often are the ring-type and linear specimens with fastened ends (Banthia et al., 1993; Yousefieh et al., 2017).

The findings of previous tests show that using PP fibres may significantly reduce the drying and overall shrinkage of concrete. Some studies (Juarez et al., 2015) have examined how employing various fibres with different aspect ratios affects the cracking characteristics.

Previous research found that adding a .2% V_f of 15 mm long PP fibre to alkali-activated slag mortar minimised drying shrinkage by 37.1%. This was achieved by adding PP fibres. In addition, there has been evidence of good bonding between the matrix and PP fibres, which is directly proportional to the enhancement of the material’s mechanical characteristics (Xu et al., 2021).

The results of a previous study (Wu et al., 2020; Rani et al., 2022) indicate that the PP fibre enhances the performance of concrete by preventing chloride penetration and extends its lifespan. The findings also show that adding PP fibres to concrete increases the resilience of the material to high-temperature exposure.

According to the findings, including fibre in the mix boosts compressive strength by 16%, 20%, and 3% at ages 3, 7, and 28 days, respectively. Additionally, it enhanced the flexural toughness index by up to 7.7 times. Further, fractures formed to their maximum depth in every single one of the concrete ring tests, except for the combination that included PP. The combination of PP fibres reduces the effect of reducing crack width by up to 62% while simultaneously enhancing age cracking by up to 84% (Saradar et al., 2018) Further, adding fibres at a relatively high volume percentage of 5% improved the compressive strength and flexural toughness of mortar specimens (McLain, 1974; Boghossian and Wegner, 2008).

An eccentric-ring geometry was used to determine the degree of early-age shrinkage cracking under restrained conditions. The initial cracking was predicted to occur earlier than that in a circular geometry to reduce the experiment duration. It was previously proven that an eccentric ring has a higher stress intensity owing to the geometrical effect (Hossain and Weiss, 2006; Dong et al., 2014).

The use of eccentric rings was proposed as a different experimental approach to detect the potential of cement-based composite cracking under hight restraint conditions and to achieve a quicker and more accurate evaluation of the cracking tendency of cementitious composites (Abusogi and Wei, 2018; Tian and Wei, 2019). The most significant distinction is that the cementitious material in the eccentric rings is placed under complex and non-uniform circumferential stress owing to the eccentricity between the outer and inner circles. The cracks in the restrained cementitious rings started at the internal circumference and progressed to the outside circumference towards the arrow side. The cracks subsequently move and propagate across the ring wall, depending on the amount of water in the cement.

To explore the mechanism of this test method in detail, previous studies utilised numerical analysis to simulate stress development and crack initiation in cementitious ring specimens under restrained-shrinkage, considering the coupling of thermal, moisture diffusion, and mechanical analyses (Abusogi and Wei, 2018; Abusogi and Wei, 2019). Thermal characteristics were used to calculate the nodal temperature. Moisture diffusion was investigated by considering the relationship between the differential equation that regularises the heat-transfer analysis and moisture diffusion. Previous research has shown the relevance of employing an eccentric-ring mould to analyse early-age shrinkage cracking (Abusogi et al., 2017; Abusogi and Bakri, 2022).

The purpose of this study was to evaluate the characteristics of restraint-drying shrinkage and mechanical strength of cementitious mortar reinforced with PP fibres at w/c ratios of .3, .4, and .5, with three different fibre V_f values of .4%, .6%, and .8%. To achieve this goal, the restraint-drying shrinkage was measured using an eccentric-ring test. The early-age cracks were assessed in the presence of a more complicated and non-uniform circumferential stress, and the effect of PP fibres was examined. The properties of drying-shrinkage cracks (crack width, age, and area) were investigated. The compressive and tensile strengths of the cement paste and mortar with fibres were examined. Finally, two variables were chosen (W/C ratio and volume fraction) as input parameters for the analysis of early-age cracking, crack width, compressive strength, and tensile strength of the cement paste and mortar with fibres. All tests were completed in an environmental test room at a temperature of 20°C and a relative humidity of 45%. All specimens were kept for 24 h in a curing room at a temperature of 20°C and a humidity of 98%, to achieve a standardised evaporation rate.

2 Materials and methods

2.1 Materials

2.1.1 Cement

All mixing in this investigation was completed using Type 1 ordinary Portland cement (OPC) of a specific gravity of 3,153 kg/m³ and a specific surface area of 3.19 m²/g. Table 1 provides a summary of the OPC chemical components. The OPC chemical composition and fineness effect shrinking (Branston et al., 2016).

TABLE 1

TABLE 1. Chemical composition of the used ordinary Portland cement (OPC).

2.1.2 Mixing water and superplasticisers (SP)

Potable water free from contaminants or impurities from a municipal tap was used for mixing and curing. High-performance solid superplasticiser type β-naphthalene and ranged from .1, .2, and .25% of cement weight with a fibre V_f of .4%, .6%, and .8% and w/c of .3 to achieve more workable enhance the workability of the fresh mortar.

2.1.3 Fine aggregate (sand)

Sieve analysis was performed according to the Chinese Standard (Zhang et al., 2006) to attain the particle size distribution of the fine aggregates utilised in this investigation, as shown in Figure 1. The sand was taken from local river sand. To get rid of any moisture that had been absorbed prior to material processing, the sand was pre-treated for 24 h in a drying oven at 105°C. Then particle size distribution was performed, confirming that the fineness modulus was three.

FIGURE 1

FIGURE 1. Cumulative (%) passing of sand particle.

2.1.4 Monofilament PP fibres

The synthetic monofilament PP fibre shown in Figure 2 was derived from monomeric hydrocarbons of a specific gravity of 910 kg/m³.

FIGURE 2

FIGURE 2. Type of PP fibre sample used.

The good mechanical properties of PP fibres offer a fracture strength greater than 400 MPa and Young’s modulus of 3.5 GPa. The mode of polymerisation gives PP a sterically regular atomic arrangement that results in its chemical inertness. Hence, it can be added to a highly alkaline matrix without any adverse effects on its properties. In this study, monofilament PP straight was proposed and added to cement mortar. Table 2 lists the characteristics of the PP fibres.

TABLE 2

TABLE 2. Geometry and mechanical characteristics of monofilament PP fibre.

2.1.5 Mixing procedure

In the mixing procedure, fine aggregates, including PP fibres, were carefully incorporated during the mixing process in a cement rotary mixer at 45 rpm for 3–4 min, after that a further 3 min were spent mixing the cement in the mixer. The remaining mixing water and Superplasticisers were then incorporated into the mixture and mixed for another 5 min before pouring into ring-shaped moulds. The specimens were covered with lids to obtain a sealed off environment that prevented evaporation.

2.2 Design of the mix

Table 3 shows the amounts of each type of mix used in this study, as well as a description of the mix that was used. The proportion of cement remained constant at 1,200 kg/m³ in all mixes. However, the sand, w/c ratio, and superplasticiser were varied based on the required mix design. The V_f of PP fibres varied from 0, .4%, .6%, and .8% based on the required mix design for the cement mortar and cement paste. For convenience, a mix code was assigned to each mix.

TABLE 3

TABLE 3. Mass proportions of mixes used.

To obtain findings that were similar to those of other researchers who used various fibres, cement-to-sand ratios of 1:2 and 1:1 were used (Lye et al., 2022). To obtain insight into the advantages of the fibre in a more practical situation, where it is probable that their impact on workability will need to be taken into consideration using a superplasticiser and a mix with a low w/c ratio of .3 was selected. As a result, the superplasticiser dosage in the above table refers to the higher dosage necessary to provide an equal flow for raising the dosage of the fibre. Using a w/c ratio of .40, a high flow mixture was developed. This mixture is useful for testing in the lab because it causes considerable shrinkage and cracking, which makes it easier to see how the fibres work. Tables 4, 5 present the proportions of each mix used in this investigation for the mortar and cement-paste mixes, respectively.

TABLE 4

TABLE 4. Fibre V_f (%) for mortar mixes.

TABLE 5

TABLE 5. Fibre V_f (%) for cement paste.

In this study, three specimen mixtures with different w/c ratios were evaluated. Each mixture had a different fibre V_f of .4%, .6%, and .8%. The mix codes are labelled according to V_f (.4%, .6%, and .8%) in percentage and mixture composite with mortar (M1, M2, and M3) and cement paste (M4, M5, and M6) with different w/c ratios. PM1, PM2, and PM3 are the plain mortar control mixes. PM4, PM5, and PM6 are the plain cement-paste control mixes with different w/c ratios without any fibre.

2.3 Experimental procedure

The specimens were cured according to ASTM standard C192. The samples were stored in a curing chamber for 24 h at 20°C and 98% humidity to maintain a standard rate of evaporation. All tests were conducted in an environmental test chamber at a temperature of 20°C and a relative humidity of 45%.

2.3.1 Mechanical-strength test

According to ASTMC1609, a tensile-strength test was performed on prismatic samples with dimensions of 160 mm × 40 mm × 40 mm. As reported in previous studies, the tests were conducted using a three-point MTS loading system with a loading rate of 50 N/s (Dalvand and Ahmadi, 2021; Abusogi and Bakri, 2022). The compressive strength was measured to investigate the strength development with respect to age. The samples were prepared, blended, and placed into a 40 mm³ × 40 mm³ × 40 mm³ mould for a compressive-strength test based on the ASTM C109 standard. A hydraulically powered material-testing system (MT810) with a loading rate of 24 kN/s (C109/C109M-16a, 2016) was used. The samples were poured and cured until their test age was attained.

2.3.2 Restrained-shrinkage test

An experiment on the early-age drying shrinkage was conducted using the eccentric-ring test, as shown in Figure 3. The purpose was to provide a new method for measuring early crack development when subjected to a more complicated and non-uniform circumferential stress in eccentric-cementitious-composite rings (Abusogi and Wei, 2019; Tian and Wei, 2019). The samples exhibited yield crack propagation owing to restraint and changes in humidity arising from self-desiccation. To study the effect of geometry, a sample of cementitious composites was cast with the outer circumference of the inner eccentric steel core. Recent studies have focused on using mortar and cement paste as the material for restraint specimens and adding different dosages of fibres (V_f ratio). In this study, mortar was used to increase the magnitude of shrinkage strain and cracking severity such that the influence of the fibre can be more readily measured. The proportions of each type of mix used in this study, along with a description of the purpose of the mixes, are listed in Table 3.

FIGURE 3

FIGURE 3. Eccentric restrained-shrinkage cracking frame.

The crack growth was slow and steady, as observed under a magnifying microscope. The crack age was recorded once it appeared on the surface of each specimen, and the largest crack width was recorded. The restrained-shrinkage test results are the computed mean values based on three specimens per recommended fibre dosage and w/c ratio.

As a result, current research has concentrated on employing mortar as the material for restraint specimens and varying the doses of fibres in relation to the V_f ratio. In this investigation, the size of the shrinkage strain and cracking severity were increased using mortar. Consequently, the impact of fibre could be measured more easily. Table 3 shows the amounts of each mix employed in this study, as well as an explanation of the mix functions. Under a magnification microscope, the fracture propagation was gradual and constant. When a crack manifested on the surface of each specimen, its age and the maximum width of the crack was immediately recorded. In this study, the results of the restricted shrinkage test are provided as the mean values computed from three specimens per suggested fibre dosage and w/c ratio.

2.4 Analysis method

To analyse the effect of the fibre-volume fraction (V_f) percentage and water-cement ratio on the relevant properties of mortar, the distance-weighted–least-squares approach was used to fit a curve to the data using the following process. Polynomial (second-order) regression was used to discover the matching Y value for each value on the X variable scale (McLain, 1974). This was performed such that the weight of each data point decreased as it moved away from the specific X value. McLain (1974) described an algorithm similar to the one used in this procedure (Rezaie et al., 2022). Multilinear regression was used to formulate the response of the tensile strength and crack width to changes in the amount of water to cement (w/c) and PP fibres [V_f (%)]. Multiple regression is an extension of ordinary least-squares (OLS) regression (Dahish et al., 2021), and uses more than one variable to describe the tensile strength and crack width in fibrous cementitious mortar.

The determination coefficient (R²) was used to evaluate the accuracy of the prediction equations, as stated in the formula below:

R^{2} = 1 - \frac{\sum_{i = 1}^{N} {(X - Y)}^{2}}{\sum_{i = 1}^{N} Y^{2}}

where X = measured from experiment and Y = multiple regression prediction.

This measure is given as a value between .0 and 1.0. If R² = 1.0 indicates a perfect fit which results in a very dependable model for future forecasts, a value of .0 would suggest that the model completely failed to formulate the data.

The Durbin–Watson statistic (DW) was applied to identify whether multicollinearity exists. This statistic can take on values ranging from 0 to 4, with a value of 2 indicating the absence of a correlation between the variables used in its calculation. Consequently, a value between 1.5 and 2.5 is suitable for building multicollinearity-free models. This section discusses mathematical expressions and models.

D W = \frac{\sum_{t = 2}^{T} (e_{t} - e_{t - 1})}{\sum_{t = 1}^{T} {e_{t}}^{2}}

where DW is the Durbin–Watson test, while e_t and e_t-1 represent the least-squares regression residuals.

3 Results and discussion

The mechanical and early-age cracking performances of fibre-cement paste and mortar are strongly dependent on the w/c ratio and dosage of fibre. This study focused on how the mechanical properties and early-age cracking shrinkage are influenced by the fibre V_f and its corresponding w/c ratio. The test results for the crack characteristics and mechanical properties with different fibre fractions for different mortar mixes are listed in Table 6.

TABLE 6

TABLE 6. Crack characteristics and mechanical properties with different fibre fractions for mortar mixes.

The test results for the crack characteristics and mechanical properties with different fibre fractions for different cement-paste mixes are listed in Table 7.

TABLE 7

TABLE 7. Crack characteristics and mechanical properties with different fibre fractions for cement-paste mixes.

3.1 Tensile strength

Results given in Table 6 show that the tensile strength increases as PP increases at a specific water-cement ratio and decreases as the water-cement ratio increases. The tensile strength of the mortar with PP fibres increased from 2.95 to 4.4 MPa as the fibre dosage increased from 0% to .8%, where the water-cement ratio was .3. When the ratio of water to cement was .4 and .5, the tensile strength increased from 1.13 to 2.09 MPa and from .029 to .75 MPa as the fibre dosage increased from 0% to .8% V_f, respectively. These results are in good agreement with previously published research studies (Wu et al., 2020; Yan et al., 2021). Figure 4 presents the effects on the tensile strength when adding fibre with different water-to-cement ratios for different mortar mixes. Figure 4 is plotted using distance-weighted least squares.

FIGURE 4

FIGURE 4. Mortar tensile strength, MPa against fibre-volume fraction, V_f (%) and water-cement (w/c) ratio.

In Figure 4, a significant effect can be seen when adding PP to the mortar. When adding .4% more V_f, the increase ranged from 26% to 53% when the ratio of water-cement ratio varied from .3 to .5. When adding .8% more V_f, the increase ranged from 54% to 110% as the water-cement ratio decreased from .5 to .3, respectively.

Figure 5 presents the effects on tensile strength when adding fibre with different water-to-cement ratios for different cement-paste mixes. In Figure 5, a significant effect of adding PP fibre to the cement paste can be evaluated. When adding .4% more V_f, the increase ranged from 9% to 32% when the ratio of water to cement went from .5 to .3. When adding .8% more V_f, the increase ranged from 32% to 68% when the ratio of water to cement decreased from .5 to .3, respectively. The magnitude of the tensile strength was highly predictive of the crack severity. However, it is evident that the advantage of fibres is not limited to their capacity to reduce the shrinking strain. The effectiveness of the fibres is attributable, at least in part, to their capacity to bridge cracks and restrict their growth.

FIGURE 5

FIGURE 5. Cement-paste tensile strength (MPa) against the fibre-volume fraction, V_f (%) and water-cement (w/c) ratio.

Table 8 presents the relevant equations for the tensile strength against the PP fibre V_f (%) and water-cement ratio for the mortar and cement-paste mixes. The values of R² present a high correlation. The DW indicates no collinearity for the tensile strengths of mortar mixes, while the cement paste DW indicates minor collinearity. These equations are limited to being used for tensile-strength response predictions of mortars and cement pastes with polypropylene fibre (V_f ≤ .8%) at a w/c ratio range from .3 to .5 in the eccentric-ring test.

TABLE 8

TABLE 8. Proposed tensile-strength equations for mortar and cement paste against PP, V_f, and w/c ranging from .3 to .5

The tensile strength increased per unit rise in PP V_f (%) was 1.472 MPa for mortar and 1.017 MPa for cement pastes. The reduction in tensile strength when the w/c ratio was increased was 11.583 MPa for mortar and 6.437 MPa for cement pastes. Thus, increasing the amount of PP fibre will provide better tensile strength, while an increase in associated w/c will weaken this enhancement.

3.2 Compressive strength

The results of the compressive strength are shown in Figure 6. The interaction between PP fibre content and the related concrete compressive strength relative to the control sample is demonstrated.

FIGURE 6

FIGURE 6. Mortar compressive strength (MPa) against fibre V_f and water-cement (w/c) ratio.

Comparison of the mixes with V_f values of .4%, .6%, and .8% showed that increasing the PP fibre enhanced the compressive strength. The rate of increase indicates a continuing upward trend in compressive strength that varies with the w/c ratio. The compressive strength of the mortar with PP fibres increases from 39.72 to 57.9 MPa (45.8%) as the fibre V_f increases from 0% to .8%, where the w/c ratio was .3. When the ratio of w/c was .4 and .5, the compressive strength increased from 24.62 to 39.66 MPa (61%) and 21.3–24.46 MPa (15%), respectively. The highest enhancement in compressive strength was associated with a lower w/c ratio of .3 with a high fibre V_f of .8%. In addition, the compressive strength increased in terms of cement-to-sand 1:2 mixtures with a w/c ratio of .4. The results agree well with the findings of a previous study (Yuan and Jia, 2021).

Figure 7 demonstrates the relationship between compressive strength (MPa) against fibre V_f and w/c ratio for the cement-paste mixes.

FIGURE 7

FIGURE 7. Cement-paste compressive strength against fibre V_f and w/c ratio.

When fibres were added to mixes to increase their strength, there was no weighty variation in compressive strength (5% increase) with a w/c ratio of .3 and V_f of .8%. When the w/c ratio was .4 and .5 with a V_f of .8%, the compressive strength increased by 9.0% and 8.3%, respectively. This is in line with other studies (Wu et al., 2020). Thus, adding PP fibres to cement pastes is insufficient to significantly affect the compressive strength. This is because the strength of concrete is determined by the bond between cement and fine or coarse aggregates.

3.3 Restrained-shrinkage cracking test

3.3.1 Crack age

The reduction in the stress development rate when the w/c ratio rises delays its cracking age. This confirms the higher crack tendency of the lower w/c ratio mixes, which is consistent with literature (Bentur and Kovler, 2003; Tian and Wei, 2019). Adding fibre to the mixtures strengthened them and delayed the appearance of cracks, as shown in Figures 8, 9 below. The crack age was detected and recorded as soon as the crack appeared on the surface of each specimen. For mortar mixtures with a low w/c ratio of .3, the cracking age was 9 days for the plain mixture (PM1). Adding .4%, .6%, and .8% V_f of PP fibres delayed the crack age by 10, 12, and 13 days, respectively. As shown in Figure 8, adding fibres delayed the crack age from 14 to 18 days and 20–23 days by adding a high Vf of .8% to PM2 and PM3, respectively.

FIGURE 8

FIGURE 8. Mortar-cracking age (days) against fibre V_f (%) and w/c ratio.

FIGURE 9

FIGURE 9. Cement-paste cracking age (h) against fibre V_f (%) and w/c ratio.

Identical results were obtained with cement-paste mixtures with .4 and .5 w/c ratios, as shown in Figure 9. Cement-paste mixtures were labelled and a w/c ratio of .3 was considered low. The first crack appeared after 32 h for the PM4. The existence of cracks propagated three to four times longer in fibre-reinforced mixes than in unreinforced mixtures. The PP dispersion fibres were the most advantageous due to their higher surface area, which results in greater frictional restraint, and their ability to bridge cracks due to the increased number of regularly spaced filaments.

3.3.2 Crack width

The results of the crack width are given in Tables 6, 7 for the mortar and cement-paste mixes, respectively. Figure 10 shows the relationship between the mortar-crack width and fibre V_f (%) and w/c ratio. Compared with plain mixtures, the crack width was reduced by 99.9% for 1:2 mix proportions by adding a V_f of .8% with a w/c ratio of .4. For a w/c ratio of .5, the cracking width was reduced by 74%–92%. The PP fibres completely decreased shrinkage cracking. The amount of fine aggregate was reduced in 1:1 mix proportions with a low w/c ratio of .3 as the volume of cement and water was increased; consequently, more strain shrinkage and cracking occurred. These results agree with those of previous studies (Alavi Nia et al., 2012).

FIGURE 10

FIGURE 10. Mortar-crack width against fibre V_f and w/c ratio.

The CRR (cracking reduction ratio) was calculated using the following equation (CWpp/CWnpp: maximum crack width of fiber mortar mixture/control mortar mixture):

C R R = 100 \times (1 - C W_{p p} / C W_{n p p})

Where

CW_pp: maximum crack width of fiber mortar mixture

CWnpp/: control mortar mixture.

Here, the effect of fibres with different V_f values might be more clearly identified. Figure 10 shows the effect of the fibre on decreasing the crack width by 60%–99% when V_f changes from .4% to .8%.

Figure 11 shows the relationship between the cement-paste crack width, fibre V_f, and w/c ratio. For cement-paste mixtures with a V_f of .4%–.8%, crack widths were reduced by 55%–78%, 58%–83%, and 50%–90% for w/c ratios of .3, .4, and .5, respectively. The plain control cement failed to meet these criteria. However, after the fibres were added, the requirements were satisfied. Hence, fibres can function as crack bridges, preventing shrinkage cracking. Table 9 shows a comparison between the cement-paste and mortar cracking widths with equal w/c ratios.

FIGURE 11

FIGURE 11. Cement-paste crack width against fibre V_f and w/c ratio.

TABLE 9

TABLE 9. Comparison between cement-paste cracking width and mortar cracking width with equal w/c ratios.

As shown in Table 9 and Figure 12, adding fine aggregates can strengthen the mixtures by reducing the amount of cement and water. The cement paste M2 and mortar M5 had the same w/c ratio of .4 and equal Vf dosages (.4–.08%). The amount of M5 fine aggregate increased the unit volume of cement and water. Since the shrinkage is largely influenced by the pore water pressure of evaporating water, this resulted in greater shrinkage strain and more cracking.

FIGURE 12

FIGURE 12. Histogram plot of crack width and fibre V_f for cement paste and mortar.

Figure 12 illustrates the cement-paste and mortar-crack widths for different fibre V_f.

Table 10 presents the relevant equations for reducing the crack widths resulting from the addition of V_f (%) and w/c ratio for all mortars and cement pastes. The R² values indicate a significant correlation, whereas the Durbin–Watson [DW] values show that these models are free from collinearity. These equations are limited to being used for prediction of the response of the crack width of mortars and cement paste with polypropylene fibre (V_f ≤ .8%) at a w/c ratio range from .3 to .5 in the eccentric-ring test. Figure 13 illustrates the reduction in crack-width percentage at different w/c ratios and fibre V_f for the mortar and cement paste.

TABLE 10

TABLE 10. Proposed equation of crack width of mortar and cement paste with PP and w/c ranging from .3 to .5 in the eccentric-ring test.

FIGURE 13

FIGURE 13. Crack-width reduction percentage at different w/c with different fibre V_f for (A) Mortar and (B) Cement paste.

The increase in crack width per unit of fibre-volume fraction V_f was reduced by 1.102% for mortar and 1.017% for cement-paste mixes. The reduction rate of crack width when the w/c ratio was increased was 1.525% for mortar, whereas it was only .061% for cement-paste mixes. As a result, increasing the amount of PP fibres would result in a better reduction in crack width, while any decrease in the associated w/c would mitigate this reduction.

3.3.3 Crack area

Figures 14A, B show the microcrack width measurement using a 100-magnification microscope and crack sample using an eccentric-ring test, respectively. Another metric used to evaluate the extent of cracking through the ring is the measurement of the cracking area. To calculate the cracking area of a ring sample, the length and breadth of all cracks were measured using a microscope with a 100-magnification. The areas of all cracks were added together.

FIGURE 14

FIGURE 14. (A) Microcrack width measurement and (B) Crack sample using the eccentric-ring test.

Figure 15 illustrates the relationship between the crack area and fibre V_f for mortar mixes with different w/c ratios.

FIGURE 15

FIGURE 15. Mortar-crack area against fibre V_f.

The scattering PP fibres reduced the cracking area for a w/c ratio of .3 by approximately 22%, 44.3%, and 83.2% for V_f values of .4%, .6%, and .8%, respectively. Contrarily, adding PP fibres reduced the cracking area by 52.8%, 82.9%, and 99.8% with .4%, .6%, and .8%, respectively for a .4 w/c ratio. The mixtures with a .5 w/c ratio demonstrated the capability of the PP fibres to limit crack growth. The reduction percentages were 77.2%, 98%, and 99.5% with V_f values of .4%, .6%, and .8%, respectively.

Figure 16 shows the relationship between the crack area and fibre (V_f) for the cement-paste mixes with different w/c ratios.

FIGURE 16

FIGURE 16. Cement-paste crack area against fibre V_f.

The addition of PP fibres to the cement paste significantly reduced the cracking area. When V_f was .2%, the crack area decreased by 40.8%, 50.6%, and 52.6% with w/c ratios of .3, .4, and .5, respectively. When the PP fibre content was .4, the reduction increased noticeably to 72.1%, 78.5%, and 95.1%. The reduction slowed when V_f was .8, reaching 99.2% at a w/c ratio of .5.

4 Conclusion

The results of this study can be summarised as follows:

1. The eccentric-ring approach more instantly reflects the cracking time, position, and other cracking parameters of the cement-mortar composites. This demonstrates how a material cracks, and the best way to study the cracking properties of fibrous mixtures is to determine how the fibres affect the crack properties.

2. This study is useful for discovering the behaviour of both restrained cement paste and mortar regarding cracking width, age, and area, and for using less prone-to-crack concrete combinations.

3. The addition of PP fibres with different V_f values to mortar and cement pastes has a substantial impact on the tensile strength. The effect of fibre dosage on V_f was estimated for different w/c ratios. The increases in tensile strength were 26%–110% and 9%–68% in the mortar and cement paste, respectively. The higher the V_f and lower the w/c ratio, the higher the tensile-strength improvement percentage.

4. Increasing the w/c ratio and amount of fine aggregates increased the cracking age.

5. Formulas for estimating the tensile strength and crack width based on the PP fibre V_f with different w/c ratios of .3–.5 were proposed. The rate of enhancement of the tensile strength or percentage of crack-width reduction was estimated.

Data availability statement

The original contributions presented in the study are included in the article/Supplementary Material, further inquiries can be directed to the corresponding authors.

Author contributions

Conceptualization and design of the research, MA; methodology, MA; formal analysis, MA, MB, and ZM; investigation, MA; resources, ZM; data curation, MA and MB; writing—original draft preparation, MA and MB; writing—review and editing, ZM and MB; visualization, MA and ZM; supervision MB and ZM; project administration, ZM and MH; funding acquisition, ZM and MH.

Conflict of interest

The authors declare that the research was conducted in the absence of any commercial or financial relationships that could be construed as a potential conflict of interest.

Publisher’s note

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Keywords: early-age shrinkage cracking, polypropylene fibres (PP), eccentric ring test, crack width, cementitious mortar

Citation: Abusogi MA, Muda ZC, Hafez MA and Bakri M (2023) Effect of polypropylene fibre on cementitious mortar early shrinkage cracking using the eccentric-ring test. Front. Mater. 9:1052870. doi: 10.3389/fmats.2022.1052870

Received: 24 September 2022; Accepted: 19 December 2022;
Published: 05 January 2023.

Edited by:

Valter Carvelli, Politecnico di Milano, Italy

Reviewed by:

Peng Zhang, Qingdao University of Technology, China
Maurizio Guadagnini, The University of Sheffield, United Kingdom

Copyright © 2023 Abusogi, Muda, Hafez and Bakri. This is an open-access article distributed under the terms of the Creative Commons Attribution License (CC BY). The use, distribution or reproduction in other forums is permitted, provided the original author(s) and the copyright owner(s) are credited and that the original publication in this journal is cited, in accordance with accepted academic practice. No use, distribution or reproduction is permitted which does not comply with these terms.

*Correspondence: Zakaria Che Muda, emFrYXJpYS5jaGVtdWRhQG5ld2ludGkuZWR1Lm15; Mudthir Bakri, bS5hbG1ha2traUBxdS5lZHUuc2E=