AUTHOR=Engels Jenni K. , Vajragupta Napat , Hartmaier Alexander TITLE=Parameterization of a Non-local Crystal Plasticity Model for Tempered Lath Martensite Using Nanoindentation and Inverse Method JOURNAL=Frontiers in Materials VOLUME=6 YEAR=2019 URL=https://www.frontiersin.org/journals/materials/articles/10.3389/fmats.2019.00247 DOI=10.3389/fmats.2019.00247 ISSN=2296-8016 ABSTRACT=

Crystal plasticity (CP) models have proven to accurately describe elasto-plastic behavior on micro- and nanometer length scales in numerous applications. However, their parameterization requires a series of experiments and inverse analysis of the results. In this regard, nanoindentation promises to be a well-suited tool for realizing a parameterization approach to determine all model parameters. The objective of this work is to develop a parameterization technique for a non-local CP model by means of an accessible and reproducible workflow. To determine its feasibility, tempered lath martensite with two different carbon contents is used as testing material. The workflow combines nanoindentation tests with finite element simulations. First, indentation into single packets of tempered lath martensitic specimen is yielding the load-displacement curves and the residual imprint topology on the surface with the help of atomic force microscopy. In a second step, a finite element simulation of the indentation using non-local crystal plasticity as constitutive model is performed with estimated model parameters. In the next step, non-local CP parameters are systematically adapted in an optimization scheme to reach optimal agreement with experiments. As a final validation step, it is successfully demonstrated that the CP model parameterized by nanoindentation is able to determine the macroscopic stress-strain response of polycrystals. Two observations are made: on the one hand, the material properties locally scatter very strongly, which is caused by fluctuations in microstructure and chemistry. On the other hand, a novel method has been demonstrated, were an inverse analysis is used to parameterize a non-local CP model for highly complex microstructures as those of tempered lath martensite. The novelty of this study is the application of nanoindentation and optimization scheme to parameterize a higher-order CP model of oligocrystals with a complex microstructure like the tempered lath martensite as well as the topology identification method developed and employed for both experiment and numerics.